HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → 1,2-Propanediamine, N-(4-nitrophenyl)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Propylenediamine | HCID 6567 | — |
| Reactant | p-Fluoronitrobenzene | HCID 9590 | — |
| Product | 1,2-Propanediamine, N-(4-nitrophenyl)- | HCID 4144414 | 92.9% |
Reaction Steps
2.8 g of 4-nitrofluorobenzene were heated to 80° C. in 29.6 g of propylenediamine and then stirred for 1 hour at the same temperature. The reaction mixture was poured into water and precipitated crystals were collected by filtration, thereby obtaining 3.6 g of N-(4-nitrophenyl)propylenediamine as crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05008267 |
| Source dataset | uspto-grants-1991_04 |
| ORD ID | ord-fc396dfd6c984906b4839b691da6d1d2 |
| Source note | uspto-grants-1991_04 |