HCID 20061242, compound → HCID 20061297, compound

HRID 1085289Notes

Reaction equation

HRID 1085289 reaction equation
[CH3:1][N:2]1[C:7]([NH:8][CH2:9][CH2:10][N:11]([CH2:19][CH2:20][CH2:21][C:22]2[CH:27]=[CH:26][C:25]([N+:28]([O-:30])=[O:29])=[CH:24][CH:23]=2)[CH2:12][C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)=[CH:6][C:5](=[O:31])[N:4]([CH3:32])[C:3]1=[O:33].[C:34]([OH:39])(=[O:38])[C:35]([OH:37])=[O:36].CO>>[C:34]([OH:39])(=[O:38])[C:35]([OH:37])=[O:36].[CH3:1][N:2]1[C:7]([NH:8][CH2:9][CH2:10][N:11]([CH2:19][CH2:20][CH2:21][C:22]2[CH:27]=[CH:26][C:25]([N+:28]([O-:30])=[O:29])=[CH:24][CH:23]=2)[CH2:12][C:13]2[CH:14]=[CH:15][CH:16]=[CH:17][CH:18]=2)=[CH:6][C:5](=[O:31])[N:4]([CH3:32])[C:3]1=[O:33]

Participants

3

Reactant 2

HCID 20061242HCID 20061242, compoundHCID 86744732HCID 86744732, compound

Product 1

HCID 20061297HCID 20061297, compound

Procedure

Further, 1.50 g of the pyrimidinedione derivative were treated in an oxalic acid/methanol solution by a method known per se in the art to obtain 1.55 g of 1,3-dimethyl-6-{2-[N-benzyl-3-(4-nitrophenyl)propylamino]ethylamino}-2,4(1H,3H)-pyrimidinedione oxalate (Compound as crystals.

Sources & evidence

ORD record
ord-058bc67606204605b97b4ab7834ede32
Source dataset
uspto-grants-1991_04
Patent number
US05008267

Reaction notes

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