Ammonia → HCID 20061874, compound

HRID 1085319Notes

Reaction equation

HRID 1085319 reaction equation
[NH3:1].[Cl:2][Ge:3]([Cl:11])([Cl:10])[CH2:4][CH2:5][S:6](Cl)(=[O:8])=[O:7]>C(Cl)(Cl)Cl>[Cl:2][Ge:3]([Cl:11])([Cl:10])[CH2:4][CH2:5][S:6]([NH2:1])(=[O:8])=[O:7]

Participants

4

Reactant 2

HCID 222AmmoniaHCID 20061872HCID 20061872, compound

Product 1

HCID 20061874HCID 20061874, compound

Reagents, catalysts & solvents 1

HCID 6212ChloroformSolvent2×

Procedure

To chloroform solution (16.0 ml) saturated with ammonia, 2-trichlorogermylethanesulfonylchloride (500 mg, obtained by Example 7) in chloroform solution (2.0 ml) was added dropwise and stirred for 22 hours at room temperature.

Sources & evidence

ORD record
ord-bffdf3e9c2cb47849488b086c1ac0a4c
Source dataset
uspto-grants-1991_04
Patent number
US05008416

Reaction notes

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