Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methyl Chloride | HCID 6327 | — |
| Reactant | 2,4,6-Trimethylbenzoyl chloride | HCID 97038 | — |
| Reactant | 6-methoxy-(6H)-dibenz[c,e][1,2]-oxaphosphorin | HCID 11436148 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 14366286 | HCID 14366286 | — |
Reaction Steps
18.25 g (0.1 mol) of 2,4,6-trimethylbenzoyl chloride were warmed to 85° C. under a nitrogen atmosphere 23 g (0.1 mol) of 6-methoxy-(6H)-dibenz[c,e][1,2]-oxaphosphorin were added dropwise while stirring. The temperature was slowly increased to 105° C. It was kept at this temperature until evolution of methyl chloride could no longer be detected. When the reaction was complete, toluene was added. After crystallization, 27 g (75% of theory) of the abovementioned compound of melting point 109° C. were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05008426 |
|---|
| Source dataset | uspto-grants-1991_04 |
|---|
| ORD ID | ord-4d8a051a351846c7a04dc09e21becb24 |
|---|
| Source note | uspto-grants-1991_04 |
|---|
