HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → 1-Bromo-8-[3-(octadecyloxy)propoxy]octane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 1,8-Dibromooctane | HCID 78310 | — |
| Reactant | 3-Octadecyloxypropanol | HCID 555303 | — |
| Catalyst | Hexadecyltrimethylammonium chloride | HCID 8154 | — |
| Product | 1-Bromo-8-[3-(octadecyloxy)propoxy]octane | HCID 20062136 | 53.1% |
Reaction Steps
Using 3-(octadecyloxy)propanol (5 g), 1,8-dibromooctane (12.7 g), cetyltrimethylammonium chloride (0.96 g) and a 50% aqueous solution of sodium hydroxide (12 g), a reaction is conducted in the same manner as that in Reference Example 4 to give the above-titled compound as colorless solid (4.2 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05008454 |
| Source dataset | uspto-grants-1991_04 |
| ORD ID | ord-d58e6cf668b34430862db0e91b59ed26 |
| Source note | uspto-grants-1991_04 |