HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → HCID 15680272, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | 2,6-Di-tert-butyl-4-mercaptophenol | HCID 70370 | — |
| Reactant | Ethyl 2-bromovalerate | HCID 79071 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 15680272 | HCID 15680272 | — |
Reaction Steps
The title compound was prepared according to the method of Example 22 from potassium hydroxide flakes (3.36 g, 0.06 mole), 2,6-bis(1,1-dimethylethyl)-4-mercaptophenol (4.76 g, 0.02 mole) and ethyl-2-bromovalerate (4.18 g, 0.02 mole) in acetone (100 ml). The structure was confirmed by NMR.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05010080 |
| Source dataset | uspto-grants-1991_04 |
| ORD ID | ord-4f0aabc2b8c04244bdacaa9ba0ce483d |
| Source note | uspto-grants-1991_04 |