HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3,6-Difluorophthalic anhydride → Ethyl 3-(4,7-difluoro-1,3-dioxo-1,3-dihydro-isoindol-2-yl)-2-(2-methyl-[1,3]dioxolan-2-yl)propionate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3,6-Difluorophthalic anhydride | HCID 513918 | — |
| Edukt | Ethyl 3-amino-2-(2-methyl-[1,3]dioxolan-2-yl)propionate | HCID 21982228 | — |
| Produkt | Ethyl 3-(4,7-difluoro-1,3-dioxo-1,3-dihydro-isoindol-2-yl)-2-(2-methyl-[1,3]dioxolan-2-yl)propionate | HCID 21982229 | — |
Reaktionsschritte
Ethyl 3-(4,7-difluoro-1,3-dioxo-1,3-dihydro-isoindol-2-yl)-2-(2-methyl-[1,3]dioxolan-2-yl)propionate was prepared in the same manner as described in the above example 5 (20) from ethyl 3-amino-2-(2-methyl-[1,3]dioxolan-2-yl)propionate (0.80 g, 3.94 mmol) and 3,6-difluorophthalic anhydride (0.94 g, 4.33 mmol), and the obtained product was identified with the following NMR data.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07094908B2 |
| Quelldatensatz | uspto-grants-2006_08 |
| ORD ID | ord-54c317bf5f6643cd8f51c9f73264cc75 |
| Quellennotiz | uspto-grants-2006_08 |