Methyl (11-oxo-6,11-dihydrodibenzo[b,e]oxepin-2-yl)acetate → HCID 12330038, compound

HRID 1085591Notes

Reaction equation

HRID 1085591 reaction equation
[O:1]=[C:2]1[C:8]2[CH:9]=[CH:10][CH:11]=[CH:12][C:7]=2[CH2:6][O:5][C:4]2[CH:13]=[CH:14][C:15]([CH2:17][C:18]([O:20][CH3:21])=[O:19])=[CH:16][C:3]1=2>C(OCC)C>[OH:1][CH:2]1[C:8]2[CH:9]=[CH:10][CH:11]=[CH:12][C:7]=2[CH2:6][O:5][C:4]2[CH:13]=[CH:14][C:15]([CH2:17][C:18]([O:20][CH3:21])=[O:19])=[CH:16][C:3]1=2

Participants

3

Reactant 1

HCID 10333952Methyl (11-oxo-6,11-dihydrodibenzo[b,e]oxepin-2-yl)acetate

Product 1

HCID 12330038HCID 12330038, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

The objective compound was obtained as light yellow crystals (recrystallized from diethyl ether) from Compound d obtained in Reference Example 4 in a manner similar to Reference Example 2.

Workup

  1. customobtained in Reference Example 4 in a manner similar to Reference Example 2

Sources & evidence

ORD record
ord-f29933b0721b4d2286fd78139f495229
Source dataset
uspto-grants-1991_04
Patent number
US05010104

Reaction notes

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