HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroquinone → 4-((11-(Acryloyloxy)undecyl)oxy)benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroquinone | HCID 785 | — |
| Reactant | Acrylic Acid | HCID 6581 | — |
| Reactant | 4-(11-hydroxyundecyloxy)benzoic acid | HCID 12297134 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | 4-((11-(Acryloyloxy)undecyl)oxy)benzoic acid | HCID 19964084 | 38.6% |
Reaction Steps
6.4 g of 4-(11-hydroxyundecanyloxy)benzoic acid and 5.8 g of acrylic acid were heat-refluxed in the pressure of hydroquinone in benzene for 80 hours. After distilling off the solvent, the product was purified by column chromatography to obtain 2.9 g of the objective product (yield: 38%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05011623 |
| Source dataset | uspto-grants-1991_04 |
| ORD ID | ord-b61c27dbb4034a67b5f7ce5bf09ea9d9 |
| Source note | uspto-grants-1991_04 |