Azobisisobutyronitrile → HCID 20058819, compound

Participants

Reaction Steps

0.500 g of 2-hexyloxypropyl 4-[4'-(11-acryloyloxyundecanoyloxy)benzoyl]benzoate and 3 mol % of azobisisobutyronitrile were added to 5 ml of dry toluene and degassed under freezing, followed by polymerization for 24 hours at 60° C. The product was repeatedly re-precipitated from methanol to obtain 0.32 g (yield: 64%) of the objective polymer, which showed the following physical properties.

Provenance & Evidence