HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzotrichloride → N,N'-Bis(4-methoxycarbonylphenyl)benzamidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzotrichloride | HCID 7367 | — |
| Reactant | Methyl 4-aminobenzoate | HCID 12082 | — |
| Product | N,N'-Bis(4-methoxycarbonylphenyl)benzamidine | HCID 15734502 | — |
Reaction Steps
N,N'-Bis(4-methoxycarbonylphenyl)benzamidine (1) was prepared from methyl 4-aminobenzoate and α,α,α-trichlorotoluene; pale-yellow crystals: mp 180°-182° C. 1H-NMR (CDCl3) 8.0-7.0 (m, 14H), 3.8 (s, 6H); IR (CDCl3) 3330, 1705, 1585; MS (m/e) 388 (M+), 238 (base).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05011628 |
| Source dataset | uspto-grants-1991_04 |
| ORD ID | ord-afa3fef6c9184771b4148ce458605d45 |
| Source note | uspto-grants-1991_04 |