Benzotrichloride → N,N'-Bis(4-n-octylcarbamylphenyl)benzamidine

Participants

Role	Name	HCID	Charge
Reactant	Benzotrichloride	HCID 7367	—
Reactant	4-amino-N-n-octylbenzamide	HCID 577709	—
Solvent	Chloroform	HCID 6212	—
Product	N,N'-Bis(4-n-octylcarbamylphenyl)benzamidine	HCID 15734504	—

Reaction Steps

N,N'-Bis(4-n-octylcarbamylphenyl)benzamidine (4) was prepared from 4-amino-N-n-octylbenzamide and α,α,α-trichlorotoluene; pale-yellow oil: 1H-NMR (CDCl3) 7.7-6.9 (m, 14H), 6.2 (br t, 2H, J=6 Hz), 3.3 (br q, 4H, J=6 Hz), 1.7-0.7 (m, 30H); IR (CHCl3) 3430, 1640, 1590; MS (m/e) 582 (M+), 335 (base).

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US05011628
Source dataset	uspto-grants-1991_04
ORD ID	ord-6250779d54df4d4fa4929c9aed463729
Source note	uspto-grants-1991_04