HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzocaine → HCID 15734512, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzocaine | HCID 2337 | — |
| Reactant | Phosphorus pentachloride | HCID 24819 | — |
| Reactant | Ethyl 4-[[4-(1,1-dimethylethyl)benzoyl]amino]benzoate | HCID 721207 | — |
| Product | HCID 15734512 | HCID 15734512 | — |
Reaction Steps
N,N'-Bis(4-ethoxycarbonylphenyl)-4-t-butylbenzamidine (14) was prepared from ethyl 4-[N-(4-t-butylbenzoyl)]aminobenzoate, phosphorus pentachloride, and ethyl 4-aminobenzoate; yellow solid: mp 212°-219° C. 1H-NMR (CDCl3) 8.0-7.0 (m, 12H), 6.0 (br s, 1H), 4.3 (q, 4H, J=7 Hz), 1.4 (t, 6H, J=7 Hz), 1.3 (s, 9H); IR (Nujol) 3330, 1710, 1590; MS (m/e) 472 (M+), 308 (base).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05011628 |
| Source dataset | uspto-grants-1991_04 |
| ORD ID | ord-ec8f284c9f0a4076a960a055abb82ac4 |
| Source note | uspto-grants-1991_04 |