HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4-Methylphthalic anhydride → Ethyl 3-(5-methyl-1,3-dioxo-1,3-dihydro-isoindol-2-yl)-2-(2-methyl-[1,3]dioxolan-2-yl)propionate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4-Methylphthalic anhydride | HCID 88069 | — |
| Edukt | Ethyl 3-amino-2-(2-methyl-[1,3]dioxolan-2-yl)propionate | HCID 21982228 | — |
| Produkt | Ethyl 3-(5-methyl-1,3-dioxo-1,3-dihydro-isoindol-2-yl)-2-(2-methyl-[1,3]dioxolan-2-yl)propionate | HCID 21982196 | — |
Reaktionsschritte
Ethyl 3-(5-methyl-1,3-dioxo-1,3-dihydro-isoindol-2-yl)-2-(2-methyl-[1,3]dioxolan-2-yl)propionate was prepared (0.38 g, 40%) in the same manner as described in the above example 5 (20) from ethyl 3-amino-2-(2-methyl-[1,3]dioxolan-2-yl)propionate (0.60 g, 3.25 mmol) and 4-methylphthalic anhydride (0.79 g, 4.87 mmol), and the obtained product was identified with the following NMR data.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07094908B2 |
| Quelldatensatz | uspto-grants-2006_08 |
| ORD ID | ord-bd672a05df5a4c7da2b20b10ff055803 |
| Quellennotiz | uspto-grants-2006_08 |