HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(4-Pyridinyl)-1-propanone → HCID 53862819, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(4-Pyridinyl)-1-propanone | HCID 74343 | — |
| Reactant | Methyl carbazate | HCID 80519 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 53862819 | HCID 53862819 | 63% |
Reaction Steps
A solution of 4.05 gm (0.03 mole) of 4-propionylpyridine, 2.70 gm (0.03 mole) of methyl carbazate and 100 ml of absolute ethanol is refluxed 6 hr. The solution is evaporated in vacuo to give a solid. The crude product is crystallized from ethyl acetate/Skellysolve B to yield 3.90 gm (63%) of the title compound having a melting point of 216.2° C. (decomp.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05011932 |
| Source dataset | uspto-grants-1991_04 |
| ORD ID | ord-aacc1d52a5a5491982776c6ec8ae629d |
| Source note | uspto-grants-1991_04 |