HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dicyclohexylcarbodiimide → HCID 178455928, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dicyclohexylcarbodiimide | HCID 10868 | — |
| Reactant | 1-Hydroxybenzotriazole | HCID 75771 | — |
| Reactant | tert-Butyl isoleucinate--hydrogen chloride (1/1) | HCID 11687228 | — |
| Reactant | HCID 178512912 | HCID 178512912 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 178455928 | HCID 178455928 | — |
Reaction Steps
2.2 g of DCC are added, at 0° C., to a stirred solution of 2.23 g of H-Ile-OtBu.HCl, 4 g (10 mmol) of Fmoc-Arg-OH and 1.35 g of HOBt in 80 ml of dimethylformamide. The working-up is carried out in analogy to Example 2b.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05011825 |
| Source dataset | uspto-grants-1991_04 |
| ORD ID | ord-a83180d7e9cb47b4bf82fc4ccc27c11a |
| Source note | uspto-grants-1991_04 |