Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | HCID 19875857 | HCID 19875857 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 19875829 | HCID 19875829 | 100% |
Reaction Steps
To a stirred solution of 30 parts of 1-(4-chloro-3-nitrophenyl)-2-methyl-1-propanone in 240 parts of methanol was added a solution of 20 parts of methanamine in 160 parts of methanol. After stirring for 12 hours at 60° C., the reaction mixture was evaporated to dry, yielding 30 parts (100%) of 2-methyl-1-[4-(methylamino)-3-nitrophenyl]-1-propanone as a residue (interm. 45).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05028606 |
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| Source dataset | uspto-grants-1991_07 |
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| ORD ID | ord-609b19c3a64d4b5598e536851008f849 |
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| Source note | uspto-grants-1991_07 |
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