Hydrazine hydrate (1:1) → HCID 14893650, compound

Participants

Reaction Steps

To a mixture of 1.27 g of 2-cyanoiminothiazolidine well-known and 20 ml of methanol was added 0.3 ml of hydrazine monohydrate, and the mixture was stirred at room temperature for an hour. After the reaction, the solvent was evaporated under reduced pressure, and the residue was recrystallized from water to give 1.42 g of bis{2-[N-(5-amino-1,2,4-triazol-3-yl)amino]ethyl}disulfide (Compound 3).

Provenance & Evidence