HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propylenediamine → HCID 178442810, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propylenediamine | HCID 6567 | — |
| Reactant | Dodecanenitrile | HCID 17092 | — |
| Solvent | Carbon Disulfide | HCID 6348 | — |
| Product | HCID 178442810 | HCID 178442810 | 75% |
Reaction Steps
18.13 g (100 mmoles) of undecyl cyanide, 9.3 g (125 mmoles) of 1,2-diaminopropane and 0.5 ml of carbon disulfide were heated to 125° C. for 24 hrs. and then worked up as mentioned under Example 23. Kugelrohr distillation at 163°-165° C./1.2-1.4 mm Hg gave 17.85 g (75%) of product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05030629 |
| Source dataset | uspto-grants-1991_07 |
| ORD ID | ord-1057eca2c9d04dafbcd0bf8bba736016 |
| Source note | uspto-grants-1991_07 |