HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hexanenitrile → HCID 178442284, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hexanenitrile | HCID 12352 | — |
| Reactant | 2-Methylpropylenediamine | HCID 13128 | — |
| Solvent | Carbon Disulfide | HCID 6348 | — |
| Product | HCID 178442284 | HCID 178442284 | 73.4% |
Reaction Steps
8.41 g (95.4 mmoles) of 1,2-diamino-2-methylpropane, 7.4 g (76.16 mmoles) of hexanenitrile and 0.4 ml of carbon disulfide were heated at 125° C. for 24 hours and then worked up as under Example 23. Distillation at 105°-107° C./0.5 mm gave 9.4 g (73.4%) of product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05030629 |
| Source dataset | uspto-grants-1991_07 |
| ORD ID | ord-774414b09cb54582b80ce98d82d5fa71 |
| Source note | uspto-grants-1991_07 |