2,6-Di-tert-butyl-4-mercaptophenol → 3-[[3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl]thio]-N-ethyl-N-(4-pyridinylmethyl)propanamide

Participants

Reaction Steps

The title compound was prepared according to the method of Example 4 from N-ethyl-N-(4-pyridinylmethyl)-2-propenamide (1.5 g, 0.00788 mole,), 2,6-bis(1,1-dimethylethyl)-4-mercaptophenol (2.06 g, 0.00867 mole,) and triethylamine (1 ml) to provide 3.0g of product, m.p. ca. 121°-123° C. Analysis calc. for C25H36N2O2S(428.63): Calc.: C, 70.05; H, 8.47; N, 6.54; S, 7.48. Found: C, 70.23; H, 8.55; N, 6.34; S, 7.55.

Provenance & Evidence