HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178472447, compound → HCID 178472448, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178472447 | HCID 178472447 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178472448 | HCID 178472448 | 97% |
Reaction Steps
3-{1-[(cis-4-Ethoxycarbonyl-cyclohexyl)carbamoyl]cyclopentyl}-2-(cyclohex-2-enyl)propanoic acid (185 mg, 0.441 mmol) was dissolved in absolute ethanol (50 ml) and hydrogenated at 50 p.s.i. (3.45 bar) over 5% palladium on charcoal (10 mg) as catalyst. The solution was filtered and the solvent evaporated to give the title compound as a colourless gum (180 mg, 97%). Found: C,65.56; H,9.05; N,3.31. C24H39NO5.H2O requires C,65.57; H,9.39; N,3.18%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05030654 |
| Source dataset | uspto-grants-1991_07 |
| ORD ID | ord-973a4b4c55f04963a6289731f8b80f65 |
| Source note | uspto-grants-1991_07 |