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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1086730Generated: October 31, 2026

HCID 178472447, compound → HCID 178472448, compound

https://huagongshe.com/reaction/1086730

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 178472447HCID 178472447—
CatalystPalladiumHCID 23938—
SolventEthanolHCID 702—
ProductHCID 178472448HCID 17847244897%

Reaction Steps

3-{1-[(cis-4-Ethoxycarbonyl-cyclohexyl)carbamoyl]cyclopentyl}-2-(cyclohex-2-enyl)propanoic acid (185 mg, 0.441 mmol) was dissolved in absolute ethanol (50 ml) and hydrogenated at 50 p.s.i. (3.45 bar) over 5% palladium on charcoal (10 mg) as catalyst. The solution was filtered and the solvent evaporated to give the title compound as a colourless gum (180 mg, 97%). Found: C,65.56; H,9.05; N,3.31. C24H39NO5.H2O requires C,65.57; H,9.39; N,3.18%.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05030654
Source datasetuspto-grants-1991_07
ORD IDord-973a4b4c55f04963a6289731f8b80f65
Source noteuspto-grants-1991_07