1-Bromo-3,4,5-trifluorobenzene → HCID 131716949, compound

HRID 1086768Notes

Reaction equation

HRID 1086768 reaction equation
C(C1C=CC([CH:11]2[CH2:16][CH2:15][C:14]([C:17]3[CH:22]=[C:21]([F:23])[C:20]([F:24])=[C:19]([F:25])[CH:18]=3)=[CH:13][CH2:12]2)=CC=1)CCC.[CH2:26]([C:30]1[CH:35]=[CH:34][C:33](C2CCC(=O)CC2)=[CH:32][CH:31]=1)[CH2:27][CH2:28][CH3:29].BrC1C=C(F)C(F)=C(F)C=1>>[CH2:26]([C:30]1[CH:35]=[CH:34][C:33]([C:13]2[C:14]([C:17]3[CH:18]=[C:19]([F:25])[C:20]([F:24])=[C:21]([F:23])[CH:22]=3)=[CH:15][CH:16]=[CH:11][CH:12]=2)=[CH:32][CH:31]=1)[CH2:27][CH2:28][CH3:29]

Participants

4

Reactant 3

HCID 6114091-Bromo-3,4,5-trifluorobenzeneHCID 15180849HCID 15180849, compoundHCID 19818176HCID 19818176, compound

Product 1

HCID 131716949HCID 131716949, compound

Procedure

Using 1-[4-(4-butylphenyl)cyclohexen-1-yl]-3,4,5-trifluorobenzene obtained by reacting 4-(4-butylphenyl)-cyclohexanone with 1-bromo-3,4,5-trifluorobenzene, as a starting raw material, 4"-butyl-3,4,5-trifluoroterphenyl was obtained in the same manner as in Example 3.

Workup

  1. customobtained

Sources & evidence

ORD record
ord-5d4099b546bb4d30b6806771666f7173
Source dataset
uspto-grants-1991_07
Patent number
US05032313

Reaction notes

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