Lithium borohydride → HCID 15166156, compound

HRID 1086809Notes

Reaction equation

[CH2:1]([C:5]1[CH:10]=[CH:9][C:8]([CH:11]([C:14]2[S:15][C:16]([CH2:20][CH2:21][CH2:22][C:23](OCC)=[O:24])=[C:17]([OH:19])[N:18]=2)[CH2:12][CH3:13])=[CH:7][CH:6]=1)[CH:2]([CH3:4])[CH3:3].[Li+].[BH4-]>>[CH2:1]([C:5]1[CH:10]=[CH:9][C:8]([CH:11]([C:14]2[S:15][C:16]([CH2:20][CH2:21][CH2:22][CH2:23][OH:24])=[C:17]([OH:19])[N:18]=2)[CH2:12][CH3:13])=[CH:7][CH:6]=1)[CH:2]([CH3:3])[CH3:4]

Participants

Reactant 2

HCID 4148881Lithium borohydride

HCID 15166154HCID 15166154, compound

Product 1

HCID 15166156HCID 15166156, compound

Procedure

The desired compound is prepared from the product of Example 19 by reduction with LiBH4.

Sources & evidence

ORD record: ord-f8c5a0bb3b444aefae4d48a736ae44ae
Source dataset: uspto-grants-1991_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05032588

Reaction notes

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