HCID 19818483, compound → HCID 19818473, compound

HRID 1086817Notes

Reaction equation

[CH2:1]([N:3]1[C:7]([CH:8]([CH3:10])[CH3:9])=[C:6]([CH2:11][CH2:12][N:13]([CH2:15][CH:16]([OH:25])[CH2:17][C:18]([O:20]C(C)(C)C)=[O:19])[OH:14])[C:5]([C:26]2[CH:31]=[CH:30][C:29]([F:32])=[CH:28][CH:27]=2)=[C:4]1[C:33]1[CH:38]=[CH:37][CH:36]=[CH:35][CH:34]=1)[CH3:2].C(Cl)(Cl)[Cl:40].CO>>[ClH:40].[CH2:1]([N:3]1[C:7]([CH:8]([CH3:9])[CH3:10])=[C:6]([CH2:11][CH2:12][N:13]([CH2:15][CH:16]([OH:25])[CH2:17][C:18]([OH:20])=[O:19])[OH:14])[C:5]([C:26]2[CH:27]=[CH:28][C:29]([F:32])=[CH:30][CH:31]=2)=[C:4]1[C:33]1[CH:38]=[CH:37][CH:36]=[CH:35][CH:34]=1)[CH3:2]

Participants

Reactant 2

HCID 19818483HCID 19818483, compound

HCID 21584188Chloroform methanol

Product 1

HCID 19818473HCID 19818473, compound

Procedure

The compound is obtained from the compound from Example 10 analogously to Example 8. Colorless foam Rf =0.2 (chloroform/methanol 5:1)

Sources & evidence

ORD record: ord-deaa5df13a394310a3fe068bfa2b3640
Source dataset: uspto-grants-1991_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05032590

Reaction notes

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