HCID 54135160, compound → HCID 53699739, compound

HRID 1086900Notes

Reaction equation

HRID 1086900 reaction equation
[O:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[CH:6]=[CH:7][CH2:8][CH2:9][CH2:10][C:11](O)=[O:12]>CCOCC>[O:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[CH:6]=[CH:7][CH2:8][CH2:9][CH2:10][CH2:11][OH:12]

Participants

3

Reactant 1

HCID 54135160HCID 54135160, compound

Product 1

HCID 53699739HCID 53699739, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

6-(2-Furyl)-5-hexenoic acid (3.6 g) in ether (25 ml) was reduced according to the method of Intermediate 15, except that the reaction time was 1.5 h, and there was no purification by FCC. The title compound was obtained as a pale yellow oil (2.89 g), t.l.c. (hexane-ether 1:1) Rf 0.17.

Workup

  1. customno purification by FCC

Sources & evidence

ORD record
ord-12462952fb8f4c2c8e4ec0c436c92635
Source dataset
uspto-grants-1991_07
Patent number
US05032609

Reaction notes

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