HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Phenylethanol → HCID 67834267, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Phenylethanol | HCID 6054 | — |
| Reactant | 2,4,6-Trimethylpyridine | HCID 7953 | — |
| Reactant | 2,4-Dimethoxybenzaldehyde | HCID 69175 | — |
| Reactant | HCID 86744914 | HCID 86744914 | — |
| Product | HCID 67834267 | HCID 67834267 | 52% |
Reaction Steps
In a manner exactly analogous to the preparation of compound 35, using 4.4 g (0.0024 mole) of cyanuric chloride (1), 2.9 g (0.0024 mole) of phenethyl alcohol and 3.2 ml of collidine, 3.37 g (52% yield) of the desired compound 46 was obtained after plug filtration of the crude product on silica gel using methylene chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05032677 |
| Source dataset | uspto-grants-1991_07 |
| ORD ID | ord-83b757da02514fdc9d17b4f672570ede |
| Source note | uspto-grants-1991_07 |