HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Chloroperbenzoic acid → 4-[(2-Hydroxyethyl(3-(propylsulfinyl)propyl)amino]butyl]benzonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | 4-[4-[(2-Hydroxyethyl)[3-(propylthio)propyl]amino]butyl]benzonitrile | HCID 15158824 | — |
| Product | 4-[(2-Hydroxyethyl(3-(propylsulfinyl)propyl)amino]butyl]benzonitrile | HCID 15158825 | 24.6% |
Reaction Steps
3.1 g of 4-[4- [(2-hydroxyethyl)[3-(propylthio)propyl]amino]butyl]benzonitrile was oxidized with 2.2 g of m-chloroperbenzoic acid in analogy with example 2. The yield was 0.8 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05034411 |
| Source dataset | uspto-grants-1991_07 |
| ORD ID | ord-bd099d4f239a467b8f2e2717ea1c9b97 |
| Source note | uspto-grants-1991_07 |