HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloromethyl hexanoate → HCID 178445524, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloromethyl hexanoate | HCID 525229 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 178527738 | HCID 178527738 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 178445524 | HCID 178445524 | — |
Reaction Steps
23.1 g hexanoic acid chloromethyl ester are added over a period of 30 minutes with stirring to 17.2 g 4-mercapto-1,2,3-triazole, sodium salt, in 100 ml dimethyl formamide. After 2 h, the mixture is added to 600 ml ice water and the oil formed is taken up in ethyl acetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05035987 |
| Source dataset | uspto-grants-1991_07 |
| ORD ID | ord-e85c571e73c74af58ee5112d07b27c71 |
| Source note | uspto-grants-1991_07 |