HCID 13151869, compound → HCID 15661031, compound

HRID 1087389Notes

Reaction equation

HRID 1087389 reaction equation
[C:1]([C:4]1[CH:23]=[CH:22][C:7]2[S:8](=[O:21])(=[O:20])[C:9]3[CH:16]=[C:15]([C:17]([OH:19])=[O:18])[CH:14]=[CH:13][C:10]=3[CH2:11][CH2:12][C:6]=2[CH:5]=1)(=[O:3])[CH3:2].[C:24](C1C=CC2SC3C=C(C(O)=O)C=CC=3CCC=2C=1)(=O)C>>[C:1]([C:4]1[CH:23]=[CH:22][C:7]2[S:8](=[O:21])(=[O:20])[C:9]3[CH:16]=[C:15]([C:17]([O:19][CH3:24])=[O:18])[CH:14]=[CH:13][C:10]=3[CH2:11][CH2:12][C:6]=2[CH:5]=1)(=[O:3])[CH3:2]

Participants

3

Reactant 2

HCID 13151869HCID 13151869, compoundHCID 13151870HCID 13151870, compound

Product 1

HCID 15661031HCID 15661031, compound

Procedure

Following the procedure described in Example 10, Step 1, but substituting 2-acetyl-5,5-dioxo-10,11-dihydrodibenzo[b,f]thiepin-7-carboxylic acid (U.S. Pat. No. 4,536,507 (1985)) for 2-acetyl-10,11-dihydrodibenzo[b,f]thiepin-7-carboxylic acid as starting material, the title product was obtained as a solid.

Sources & evidence

ORD record
ord-9cd43175124a427090a7cc7b5fa2a728
Source dataset
uspto-grants-1991_07
Patent number
US05036067

Reaction notes

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