Methoxymethyl-triphenylphosphonium chloride → HCID 54282408, compound

HRID 1087398Notes

Reaction equation

HRID 1087398 reaction equation
[Cl:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[CH:9]([CH2:18][CH3:19])[C:10]([C:12]1[CH:13]=[N:14][CH:15]=[CH:16][CH:17]=1)=O.[Cl-].[CH3:21][O:22][CH2:23][P+](C1C=CC=CC=1)(C1C=CC=CC=1)C1C=CC=CC=1>>[Cl:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[CH:9]([CH2:18][CH3:19])[C:10]([C:12]1[CH:13]=[N:14][CH:15]=[CH:16][CH:17]=1)=[CH:21][O:22][CH3:23]

Participants

3

Reactant 2

HCID 2723798Methoxymethyl-triphenylphosphonium chlorideHCID 19817052HCID 19817052, compound

Product 1

HCID 54282408HCID 54282408, compound

Procedure

starting from 2-(2,4-dichlorophenyl)-1-(3-pyridyl)-1-butanone and methoxymethyltriphenylphosphonium chloride there is obtained 3-(2,4-dichloro-β-ethyl-α-methoxymethylenephenethyl)-pyridine as an isomer mixture in the form of a yellow oil;

Sources & evidence

ORD record
ord-579457c423e84bddb0fea472f2c5d481
Source dataset
uspto-grants-1991_07
Patent number
US05036074

Reaction notes

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