HuagongsheHuagongshe Chemistry Print Report · For research reference only
Epichlorohydrin → HCID 19817112, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Epichlorohydrin | HCID 7835 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-Bromothiophenol | HCID 66049 | — |
| Solvent | Methyl Ethyl Ketone | HCID 6569 | — |
| Product | HCID 19817112 | HCID 19817112 | — |
Reaction Steps
A suspension containing 9.45 g of 4-bromothiophenol, 14.45 g of 1-chloro-2,3-epoxypropane and 13.8 g of potassium carbonate in 100 ml of butanone is refluxed for 12 hours. The inorganic salts formed are filtered off and drained and the solvent and excess 1-chloro-2,3-epoxypropane are then evaporated off under vacuum. The residual oil is distilled at between 130° C. and 140° C. under 0.01 mm of mercury.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05036077 |
| Source dataset | uspto-grants-1991_07 |
| ORD ID | ord-caa35dd0ddbd4d70b3a9e8a93ae5a47f |
| Source note | uspto-grants-1991_07 |