Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | 2-Bromo-1-(2,4-dichlorophenyl)ethan-1-one | HCID 75828 | — |
| Reactant | HCID 19817164 | HCID 19817164 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 19817170 | HCID 19817170 | — |
Reaction Steps
A mixture of 4-(1,1,2,2-tetrafluoroethoxy)methyl-2,2-dimethyl-1,3-dioxolane (6.8 g), 2-bromo-1-(2,4-dichlorophenyl)ethanone (6 g.), sulphuric acid (0.3 ml at 96%) is heated at 120° C. for 3 hours, the acetone being formed in the reaction being distilled off.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05036094 |
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| Source dataset | uspto-grants-1991_07 |
|---|
| ORD ID | ord-a707cae50158456a8d206a8debdb1ef6 |
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| Source note | uspto-grants-1991_07 |
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