HuagongsheHuagongshe Chemistry Print Report · For research reference only
Gamma-Butyrolactone → N-Decyl-4-hydroxybutyramide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Gamma-Butyrolactone | HCID 7302 | — |
| Reactant | Decylamine | HCID 8916 | — |
| Catalyst | Zincchloride | HCID 3007855 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | N-Decyl-4-hydroxybutyramide | HCID 11139345 | 44.6% |
Reaction Steps
A mixture of 15 g of decylamine, 5.48 g of gamma butyrolactone, 100 ml of toluene, and 20 mg of zinc chloride was refluxed under nitrogen for 4 days. Upon cooling the reaction mixture formed a precipitate which was recrystallized from toluene to yield 6.91 g (44.6%) of N-decyl-4-hydroxybutyramide, m.p. 74°-75° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05036152 |
| Source dataset | uspto-grants-1991_07 |
| ORD ID | ord-8b3234b006154ed18b391fb126be063d |
| Source note | uspto-grants-1991_07 |