Methylhydroxylamine → HCID 86744247, compound

HRID 1087793Notes

Reaction equation

[CH3:1][C:2]1[CH:7]=[CH:6][CH:5]=[C:4]([CH3:8])[C:3]=1[N:9]1[CH:13]=[CH:12][C:11](/[C:14](/[CH3:19])=[CH:15]\[C:16](O)=[O:17])=[CH:10]1.[CH3:20][NH:21][OH:22]>>[CH3:1][C:2]1[CH:7]=[CH:6][CH:5]=[C:4]([CH3:8])[C:3]=1[N:9]1[CH:13]=[CH:12][C:11](/[C:14](/[CH3:19])=[CH:15]\[C:16]([N:21]([OH:22])[CH3:20])=[O:17])=[CH:10]1

Participants

Reactant 2

HCID 11647Methylhydroxylamine

HCID 70359744HCID 70359744, compound

Product 1

HCID 86744247HCID 86744247, compound

Procedure

Condensation of (Z)-3-[1-(2,6-dimethylphenyl)-1H-pyrrol-3-yl]-2-butenoic acid is condensed with N-methylhydroxylamine as described in example 1(a) to yield (Z)-3-[1-(2,6-dimethylphenyl)-1H-pyrrol-3-yl]-N-hydroxy-N-methyl-2-butenamide, m.p. 158°-160°.

Sources & evidence

ORD record: ord-da941d8db0494ee19935ca86646f986a
Source dataset: uspto-grants-1990_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04960787

Reaction notes

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