HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Dimethylaniline → 1-(2,6-dimethylphenyl)-1H-pyrrole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Dimethylaniline | HCID 6896 | — |
| Reactant | 2,5-Dimethoxytetrahydrofuran | HCID 79098 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 1-(2,6-dimethylphenyl)-1H-pyrrole | HCID 4715342 | — |
Reaction Steps
A solution of 2,6-dimethylaniline (60.5 g), glacial acetic acid (600 ml) and 2,5-dimethoxytetrahydrofuran (572 g) is refluxed for 5 hours. The solvent is evaporated at 60° and reduced pressure to give 1-(2,6-dimethylphenyl)-1H-pyrrole as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04960787 |
| Source dataset | uspto-grants-1990_10 |
| ORD ID | ord-c71b3965faba4bda9f026c6549e3f676 |
| Source note | uspto-grants-1990_10 |