化工社化工社 化学情報印刷レポート · 研究参考用
4-(3-Methoxyphenyl)but-3-en-2-one → 4-(3-Methoxyphenyl)butan-2-one
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-(3-Methoxyphenyl)but-3-en-2-one | HCID 182007 | — |
| 触媒 | Palladium | HCID 23938 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | 4-(3-Methoxyphenyl)butan-2-one | HCID 11423902 | 99.2% |
反応手順
A solution of 30.1 g of 4-(3-methoxyphenyl)-3-buten-2-one in 200 ml of MeOH was hydrogenated over 200 mg of 10% palladium on carbon for two hours. The catalyst was filtered and the solvent evaporated in vacuo to give 30.2 g of yellow oily 4-(3-methoxyphenyl)-2-butanone.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04960798 |
| 出典データセット | uspto-grants-1990_10 |
| ORD ID | ord-1801c56281b94056aed1d763b7f70e4b |
| 出典メモ | uspto-grants-1990_10 |