2-Chloro-5-nitropyridine → HCID 53951174, compound

HRID 1087863Notes

Reaction equation

HRID 1087863 reaction equation
[CH3:1][O:2][C:3]([C:5]1[N:6]=[CH:7][C:8]2[NH:9][C:10]3[C:15]([C:16]=2[CH:17]=1)=[CH:14][C:13]([OH:18])=[CH:12][CH:11]=3)=[O:4].Cl[C:20]1[CH:25]=[CH:24][C:23]([N+:26]([O-:28])=[O:27])=[CH:22][N:21]=1>>[CH3:1][O:2][C:3]([C:5]1[N:6]=[CH:7][C:8]2[NH:9][C:10]3[C:15]([C:16]=2[CH:17]=1)=[CH:14][C:13]([O:18][C:20]1[CH:25]=[CH:24][C:23]([N+:26]([O-:28])=[O:27])=[CH:22][N:21]=1)=[CH:12][CH:11]=3)=[O:4]

Participants

3

Reactant 2

HCID 783082-Chloro-5-nitropyridineHCID 12789153HCID 12789153, compound

Product 1

HCID 53951174HCID 53951174, compound

Procedure

In analogy to Example 8 from 6-hydroxy-β-carboline-3-carboxylic acid methyl ester and 2-chloro-5-nitropyridine, mp 150°-155° C.

Sources & evidence

ORD record
ord-74809c48b365420f9ec5d7c79bea3412
Source dataset
uspto-grants-1990_10
Patent number
US04960777

Reaction notes

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