Hydrochloric Acid → HCID 15598744, compound

Participants

Reaction Conditions

Reaction Steps

Ethyl 4',5,7-trihydroxy-2-isoflavonecarboxylate (100 mg) was added to 10 ml of isopropanol saturated with HCl gas, and the mixture was heated at 70° C. with stirring for five hours. The solvent was distilled off under reduced pressure, the residue was purified by silica gel column chromatography (eluent:chloroform), and the solid thus obtained was recrystallized from a chlorofor/methanol mixed solvent, giving 60 mg of isopropyl 4',5,7-trihydroxy-2-isoflavonecarboxylate.

Provenance & Evidence