Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 3-Fluorophenol | HCID 9743 | — |
| Reactant | Cyclopropanecarbonyl chloride | HCID 77637 | — |
| Product | HCID 15096980 | HCID 15096980 | 98% |
Reaction Steps
To 31.4 parts of 3-fluorophenol were added dropwise 29.3 parts of cyclopropanecarbonyl chloride at 80° C. Upon completion, the whole was stirred for 1 hour at 80° C. The reaction mixture was distilled, yielding 49.7 parts (98%) of (3-fluorophenyl)cyclopropanecarboxylate; bp. 75°-85° C. at 0.5 mm. pressure (intermediate 86).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04962115 |
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| Source dataset | uspto-grants-1990_10 |
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| ORD ID | ord-c3e415bc268e44c2996d136b0ff175df |
|---|
| Source note | uspto-grants-1990_10 |
|---|
