HRID1088423

反应详情

EQUATION

反应方程式

HRID 1088423 的结构方程式

PROCEDURE

实验过程

α,α'-bis-(2-propenylphenoxy)-meta-xylene is prepared in a process similar to Example I, except that 383 grams (2.86 mole) of propenylphenol is employed along with 250 grams (1.43 moles) of α,α'-dichloro-meta-xylene to give a reaction product extracted with methylene chloride, washed with potassium hydroxide and dried over magnesium sulfate, then vaccum distilled at 80° C. to yield 407 grams of a viscous liquid (80% yield).

WORKUP

后处理

  1. customto give a reaction product
  2. extractionextracted with methylene chloride
  3. washwashed with potassium hydroxide
  4. dry with materialdried over magnesium sulfate
  5. distillationvaccum distilled at 80° C.