HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53874104, compound → HCID 22163094, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53874104 | HCID 53874104 | — |
| Catalyst | Platinum oxide (PtO) | HCID 82844 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 22163094 | HCID 22163094 | — |
Reaction Steps
A mixture of 3-methoxy-5-(1-propenyl)benzaldehyde (1.6 g) and platinum oxide (150 mg) in ethyl acetate (150 ml) were hydrogenated at 16 psi in a Parr hydrogenator for 5 hours. The mixture was filtered through a celite/charcoal plug and evaporated. Purification of the residue by flash chromatography using 12% ethyl acetate in hexane afforded the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04962203 |
| Source dataset | uspto-grants-1990_10 |
| ORD ID | ord-8d1e149263544fd9a638875247045743 |
| Source note | uspto-grants-1990_10 |