HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tributyltin azide → HCID 178466210, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tributyltin azide | HCID 4984872 | — |
| Reactant | HCID 22163119 | HCID 22163119 | — |
| Solvent | HCID 21906519 | HCID 21906519 | — |
| Product | HCID 178466210 | HCID 178466210 | — |
Reaction Steps
A mixture of tributyltin azide (1.603 g, 1.5 eg.) and the nitrile (Step 4) (1.115 g, 3.20 mmoles) was heated at 120° C. for 4 hours. Flash chromatography of this reaction mixture using EtOAc: toluene AcOH 20:80:1 and 40:60:1 yielded the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04962203 |
| Source dataset | uspto-grants-1990_10 |
| ORD ID | ord-966c7ca0c60848cbb513d2bb20ad0238 |
| Source note | uspto-grants-1990_10 |