Glycerol → HCID 21889647, compound

HRID 1088496Notes

Reaction equation

[CH2:1]1[O:4][CH:2]1[CH3:3].[OH:5][CH2:6][CH:7]([CH2:9][OH:10])[OH:8]>>[OH:5][CH2:6][CH:7]([CH2:9][OH:10])[OH:8].[CH2:1]1[O:4][CH:2]1[CH3:3]

Participants

Reactant 2

HCID 753Glycerol

HCID 6378Propylene Oxide

Product 1

HCID 21889647HCID 21889647, compound

Conditions

Temperature: 100 °C

Procedure

Calcined hydrotalcite (2.9 g), a glycerol initiated propylene oxide polyol (29.3 g, molecular weight 450) and propylene oxide (5.1 g) are combined in a 75-ml stainless steel reactor, (the reactor is purged with nitrogen) and heated to 100° C. All of the propylene oxide reacts to produce a glycerol-propylene oxide adduct.

Workup

customare combined in a 75-ml stainless steel reactor
custom(the reactor is purged with nitrogen) and
customAll of the propylene oxide reacts

Sources & evidence

ORD record: ord-447f3b88d52a4f60bed2240b3a0e483d
Source dataset: uspto-grants-1990_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04962237

Reaction notes

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