Pyridine → HCID 57176419, compound

HRID 1088497Notes

Reaction equation

HRID 1088497 reaction equation
[CH2:1]([C:10]1[CH:15]=[CH:14][C:13]([C:16](=O)[CH3:17])=[CH:12][CH:11]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH3:9].[NH2:19][C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1.C1(C)C=CC=CC=1.N1C=CC=CC=1>O>[CH3:17][C:16](=[N:19][C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1)[C:13]1[CH:14]=[CH:15][C:10]([CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH3:9])=[CH:11][CH:12]=1

Participants

6

Reactant 4

HCID 1049PyridineHCID 1140TolueneHCID 6115AnilineHCID 142175p-Nonylacetophenone

Product 1

HCID 57176419HCID 57176419, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

A solution of p-nonyl acetophenone (90 g), aniline (75 g), Toluene (125 ml) and pyridine (20 ml) was refluxed with continuous removal of water. N-(alpha-methyl-p-nonyl benzylidene) aniline (XXX) was obtained by fractional distillation. XXX had a boiling point of 200°-208° at 0.075 millimeter.

Sources & evidence

ORD record
ord-d10dd96a9cd8473cb7acd20ab2f3978c
Source dataset
uspto-grants-1990_10
Patent number
US04962234

Reaction notes

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