HCID 57176419, compound → HCID 22163143, compound

HRID 1088498Notes

Reaction equation

HRID 1088498 reaction equation
[CH3:1][C:2](=[N:18][C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1)[C:3]1[CH:8]=[CH:7][C:6]([CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH3:17])=[CH:5][CH:4]=1>[Pd].C(O)C>[CH3:1][CH:2]([NH:18][C:19]1[CH:20]=[CH:21][CH:22]=[CH:23][CH:24]=1)[C:3]1[CH:8]=[CH:7][C:6]([CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH3:17])=[CH:5][CH:4]=1

Participants

4

Reactant 1

HCID 57176419HCID 57176419, compound

Product 1

HCID 22163143HCID 22163143, compound

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 702EthanolSolvent

Procedure

N-alpha-methyl-p-nonyl benzylidene) aniline (XXX) (40 g) prepared by the procedure described in Example XVI A was hydrogenated using 5% Pd/C as the catalyst and 95% ethanol as the solvent. N-(alpha-methyl-p-nonyl benzyl) aniline (XXXI) was obtained by fractional distillation. XXXI had a boiling point of 183° C. at 0.15 millimeter.

Sources & evidence

ORD record
ord-bafbe4478deb4414891b5a1fe2a80221
Source dataset
uspto-grants-1990_10
Patent number
US04962234

Reaction notes

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