HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene → N-(alpha-methyl benzylidene)-p-dodecyl aniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene | HCID 241 | — |
| Reactant | Acetophenone | HCID 7410 | — |
| Reactant | 4-Dodecylaniline | HCID 7701 | — |
| Solvent | Water | HCID 962 | — |
| Product | N-(alpha-methyl benzylidene)-p-dodecyl aniline | HCID 53927130 | 93.7% |
Reaction Steps
solution of acetophenone (33.5 g), p-dodecyl aniline (73 g), benzene (50 ml) was refluxed in the presence of molecular sieve (100 g) with continuous removal of water. The crude product was purified by crystallizing it from ethanol to give N-(α-methyl benzylidene)-p-dodecyl aniline (V) (95 g). V had a melting point of 47° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04962234 |
| Source dataset | uspto-grants-1990_10 |
| ORD ID | ord-0b58fc5e02bd472c8f16da3fc2be4448 |
| Source note | uspto-grants-1990_10 |