HCID 53927130, compound → HCID 22163144, compound

HRID 1088503Notes

Reaction equation

HRID 1088503 reaction equation
[CH3:1][C:2](=[N:9][C:10]1[CH:15]=[CH:14][C:13]([CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH3:27])=[CH:12][CH:11]=1)[C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1>[Pd].C(O)C>[CH3:1][CH:2]([NH:9][C:10]1[CH:11]=[CH:12][C:13]([CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH3:27])=[CH:14][CH:15]=1)[C:3]1[CH:4]=[CH:5][CH:6]=[CH:7][CH:8]=1

Participants

4

Reactant 1

HCID 53927130HCID 53927130, compound

Product 1

HCID 22163144HCID 22163144, compound

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 702EthanolSolvent

Procedure

N-(α-methyl benzylidene)-p-dodecyl aniline (80 g) prepared by the procedure described in Example IIIA was hydrogenated using 5% Pd/C as the catalyst and 95% ethanol as the solvent to give N-(α-methyl benzyl)-p-dodecyl aniline (VI). VI had a boiling point of 188° C. at 0.03 millimeter.

Sources & evidence

ORD record
ord-2bd3cf42726a434282b3b72d4e83437c
Source dataset
uspto-grants-1990_10
Patent number
US04962234

Reaction notes

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