HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene → 2743-00-2
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene | HCID 241 | — |
| Reactant | Acetophenone | HCID 7410 | — |
| Reactant | P-Anisidine | HCID 7732 | — |
| Solvent | Water | HCID 962 | — |
| Product | 2743-00-2 | HCID 3831695 | — |
Reaction Steps
A solution of acetophenone (64 ml), p-anisidine (65 mg), benzene (100 ml) was refluxed in the presence of molecular sieve (100 g) with continuous removal of water. The crude product was purified by crystallizing it from ethanol to give N-(αmethyl-benzylidene)-p-anisidine (VII) (50 g). VII had a melting point of 81°-82° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04962234 |
| Source dataset | uspto-grants-1990_10 |
| ORD ID | ord-2a2fc40be80a4e3baeb746a53558c36c |
| Source note | uspto-grants-1990_10 |