2743-00-2 → 4-methoxy-N-(1-phenylethyl)aniline

HRID 1088505Notes

Reaction equation

HRID 1088505 reaction equation
[CH3:1][C:2](=[N:9][C:10]1[CH:17]=[CH:16][C:13]([O:14][CH3:15])=[CH:12][CH:11]=1)[C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1>[Pd].C(O)C>[CH3:1][CH:2]([NH:9][C:10]1[CH:11]=[CH:12][C:13]([O:14][CH3:15])=[CH:16][CH:17]=1)[C:3]1[CH:4]=[CH:5][CH:6]=[CH:7][CH:8]=1

Participants

4

Reactant 1

HCID 38316952743-00-2

Product 1

HCID 38497614-methoxy-N-(1-phenylethyl)aniline

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 702EthanolSolvent

Procedure

N-(α-methyl benzylidene)-p-anisidine (VII) prepared by the procedure described in example IVA was hydrogenated using 5% Pd/C as the catalyst and 95% ethanol as the solvent to give N-(α-methyl benzyl)-p-anisidine (VIII). VIII had a melting point of 64° C.

Sources & evidence

ORD record
ord-990c9f0965de46ed97d93738c6c29c8a
Source dataset
uspto-grants-1990_10
Patent number
US04962234

Reaction notes

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